Ceramics-Silikáty 48, (3) 85 - 92 (2004) |
|
HYDROTHERMAL AGEING OF TETRAGONAL ZIRCONIA CERAMICS |
Částková Klára, Hadraba Hynek, Cihlář Jaroslav |
Department of Ceramics, Brno University of Technology,
Technická 2, 619 69 Brno, Czech Republic
|
Keywords: Zirconia, Hydrothermal ageing, Phase transformation, Mechanical properties |
The effect of hydrothermal treatment on the phase stability, microstructure and mechanical properties of tetragonal zirconia
ceramics stabilized with 3 mol% yttria was studied. At temperatures of 140-260°C the tetragonal phase transformed into monoclinic
zirconia. The degree of transformation increased with increasing temperature and time of ageing. Changes in the
microstructure and mechanical properties were observed for the samples used at temperatures of 180°C and higher. The thickness
of transformed layer increased with increasing temperature and at 260°C it reached a thickness of 170 µm after 10 hours.
The changes in mechanical properties (hardness and fracture toughness) corresponded to the structural changes in the material
caused by hydrothermal ageing. Temperatures of 180°C and higher were critical for the mechanical and structural properties
of the material. |
PDF (0.4 MB) |
|